. 2019 Sep 27;10(44):10417–10421. doi: 10.1039/c9sc04177j

Table 4. Hydroalkenylation of dienes with α,β-unsaturated hydrazones ^a .

graphic file with name c9sc04177j-u4.jpg

^aReaction conditions: 1a (0.4 mmol), α,β-unsaturated hydrazones 4 (0.2 mmol), Ni(COD)₂ (0.02 mmol), P(4-CF₃C₆H₄)₃ (0.024 mmol), ^tBuOLi (0.02 mmol), EtOH (1.5 mL) at 80 °C for 8 h. Isolated yields. Regioselectivity was determined by ¹H NMR analysis.

^b 1a (0.2 mmol), α,β-unsaturated hydrazones 4 (0.4 mmol).

Table 4. Hydroalkenylation of dienes with α,β-unsaturated hydrazones a .

Table 4. Hydroalkenylation of dienes with α,β-unsaturated hydrazones ^a .