Table 3.
position | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | 11 |
---|---|---|---|---|---|---|---|---|---|---|---|
1 | 203.8 C | 204.1 C | 203.3 C | 211.0 C | 203.5 C | 202.9 C | 202.8 C | 203.7 C | 209.9 C | 204.2 C | 203.0 C |
2 | 129.2 CH | 127.9 CH | 129.3 CH | 39.8 CH2 | 129.4 CH | 129.8 CH | 130.0 CH | 127.9 CH | 39.6 CH2 | 128.0 CH | 129.9 CH |
3 | 144.7 CH | 145.3 CH | 144.3 CH | 126.8 CH | 144.3CH | 143.6 CH | 143.5 CH | 144.9 CH | 123.9 CH | 145.3 CH | 143.7 CH |
4 | 33.0 CH2 | 33.4 CH2 | 33.0 CH2 | 129.2 CH | 33.0 CH2 | 32.9 CH2 | 32.8 CH2 | 32.8 CH2 | 128.6 CH | 33.5 CH2 | 32.8 CH2 |
5 | 62.1 C | 135.2 C | 62.1 C | 141.0 C | 61.9 C | 62.2 C | 62.2 C | 136.3 C | 141.6 C | 135.1 C | 62.1 C |
6 | 64.0 CH | 124.8 CH | 63.2 CH | 121.9 CH | 64.0 CH | 64.1 CH | 63.8 CH | 129.8 CH | 130.7 CH | 125.0 CH | 64.1 CH |
7 | 26.3 CH2 | 25.3 CH2 | 30.9 CH2 | 25.8 CH2 | 26.2 CH2 | 26.3 CH2 | 26.0 CH2 | 65.9 CH | 66.3 CH | 25.3 CH2 | 26.2 CH2 |
8 | 34.0 CH | 35.1 CH | 28.5 CH | 35.6 CH | 32.3 CH | 34.1 CH | 31.2 CH | 45.1 CH | 44.4 CH | 35.3 CH | 34.1 CH |
9 | 36.9 CH | 36.3 CH | 44.9 CH | 34.1 CH | 37.4 CH | 36.7 CH | 37.0 CH | 34.4 CH | 33.3 CH | 36.2 CH | 36.8 CH |
10 | 48.5, C | 50.8 C | 48.5 C | 52.4 C | 48.5 C | 48.6 C | 48.6 C | 50.2 C | 52.0 C | 50.7 C | 48.6 C |
11 | 23.2 CH2 | 22.1 CH2 | 23.4 CH2 | 21.7 CH2 | 22.4 CH2 | 22.7 CH2 | 21.8 CH2 | 22.8 CH2 | 21.6 CH2 | 22.2 CH2 | 22.9 CH2 |
12 | 30.0 CH2 | 32.5 CH2 | 36.0 CH2 | 32.3 CH2 | 32.1 CH2 | 30.1 CH2 | 28.4 CH2 | 30.2 CH2 | 30.0 CH2 | 32.3 CH2 | 30.4 CH2 |
13 | 54.2 C | 47.4 C | 46.9 C | 54.6 C | 47.6 C | 54.8 C | 52.3 C | 54.8 C | 54.9 C | 47.3 C | 54.7 C |
14 | 83.2 C | 84.6 C | 58.1 CH | 83.7 C | 84.9 C | 82.1 C | 84.5 C | 81.7 C | 81.4 C | 84.4 C | 81.9 C |
15 | 32.5 CH2 | 32.0 CH2 | 30.9 CH2 | 31.6 CH2 | 32.5 CH2 | 32.3 CH2 | 39.9 CH2 | 34.9 CH2 | 34.6 CH2 | 32.2 CH2 | 32.4 CH2 |
16 | 37.6 CH2 | 20.9 CH2 | 126.9 CH | 37.7 CH2 | 21.3 CH2 | 37.8 CH2 | 124.3 CH | 37.6 CH2 | 37.7 CH2 | 20.8 CH2 | 37.8 CH2 |
17 | 88.3 C | 49.4 CH | 158.9 C | 88.3 C | 49.0 CH | 88.1 C | 156.4 C | 86.7 C | 86.9 C | 49.8 CH | 87.7 C |
18 | 20.6 CH3 | 17.4 CH3 | 17.9 CH3 | 20.6 CH3 | 17.5 CH3 | 20.4 CH3 | 20.6 CH3 | 20.5 CH3 | 20.5 CH3 | 17.7 CH3 | 20.6 CH3 |
19 | 15.2 CH3 | 18.9 CH3 | 14.9 CH3 | 20.2 CH3 | 15.2 CH3 | 14.6 CH3 | 14.2 CH3 | 18.5 CH3 | 19.9 CH3 | 18.9 C | 14.5 CH3 |
20 | 78.5 C | 77.5 CH | 76.7 C | 79.0 C | 77.1 C | 79.5 C | 74.7 C | 78.6 C | 78.6 C | 77.2 C | 79.2 C |
21 | 19.3 CH3 | 20.2 CH3 | 23.1 CH3 | 19.0 CH3 | 24.1 CH3 | 19.3 CH3 | 22.41 CH3 | 19.1 CH3 | 19.2 CH3 | 20.8 CH3 | 17.2 CH3 |
22 | 72.3 CH | 75.2 CH | 74.6 CH | 72.6 CH | 85.6 CH | 82.4 CH | 79.4 CH | 80.7 CH | 80.5 CH | 76.7 CH | 78.9 CH |
23 | 31.9, CH2 | 28.8 CH2 | 27.3 CH2 | 29.9 CH2 | 67.1 CH | 66.4 CH | 29.8 CH2 | 34.3 CH2 | 34.3 CH2 | 81.4 CH | 33.2 CH2 |
24 | 38.1 CH | 38.1 CH | 37.9 CH | 38.1 CH | 151.7 C | 153.4 C | 149.3 C | 151.3 C | 151.2 C | 37.2 CH | 31.8, CH |
25 | 37.7 CH | 37.7 CH | 37.9 CH | 37.8 CH | 121.9 C | 121.1 C | 127.6 C | 121.1 C | 121.2 C | 49.6 CH | 40.7 CH |
26 | 180.8 C | 180.4 C | 180.3 C | 180.8 C | 164.1 C | 164.2 C | 165.2 C | 167.2 C | 167.0 C | 177.8 C | 175.4 C |
27 | 10.5 CH3 | 10.5 CH3 | 10.5 CH3 | 10.6 CH3 | 12.9 CH3 | 12.8 CH3 | 12.4 CH3 | 12.1 CH3 | 12.2 CH3 | 14.3 CH3 | 14.4 CH3 |
28 | 72.5 CH2 | 72.2 CH2 | 72.4 CH2 | 73.0 CH2 | 15.7 CH3 | 15.5 CH3 | 22.4 CH3 | 20.6 CH3 | 20.6 CH3 | 63.2 CH2 | 21.4 CH3 |
Assignments based on DEPT, HSQC, and HMBC data.
Assignments are interchangeable.