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Fig. 3. (a) Low resolution TEM image of PNR31-b-PRc49 micelles via ROMPI-CDSA; the inset shows the high resolution image; the statistical plots show data of lengths and aspect ratios; (b) high-resolution TEM image of PNR31-b-PRc49 micelles formed after polymerization, the inset image shows the SAED pattern; (c) AFM height image and profile of PNR31-b-PRc49 micelles; the height profile is from the indicated dash line; (d) a schematic diagram illustrating the chain folding of the crystalline PRc core. The stick-ball structure indicates the possible alignment of PRc segment along the perpendicular direction.