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. 2019 Nov 29;9(12):806. doi: 10.3390/biom9120806

Table 1.

1H (500 MHz) and 13C NMR (125 MHz) data of compounds 1 and 2.

Position 1 (in Acetone-d6) 2 (in CD3OD)
δ C δH Multi (J in Hz) δ C δH Multi (J in Hz)
1 129.8 127.0
2 136.9 130.1
3 116.9 6.60 s 117.1 6.55 s
4 145.1 145.5
5 145.3 145.7
6 115.7 6.72 s 117.0 6.64 s
7 29.0 3.86 d (23.0) 39.6 2.83 d (14.5)
3.62 overlapped 2.67 d (14.5)
8 160.9 78.0
9 72.4 4.97 d (17.0) 80.1 4.17 d (10.0)
4.89 d (17.0) 3.93 d (10.0)
1′ 123.0 135.5
2′ 116.2 6.59 d (2.0) 116.0 6.58 d (2.0)
3′ 145.9 146.3
4′ 144.6 144.8
5′ 116.1 6.63 d (8.0) 116.2 6.68 d (8.0)
6′ 120.3 6.45 dd (8.0, 2.0) 120.2 6.52 dd (8.0, 2.0)
7′ 42.3 4.53 s 47.4 4.18 d (3.0)
8′ 128.2 56.2 3.24 d (3.0)
9′ 173.9 181.0