Table 1.
Position | 1 (in Acetone-d6) | 2 (in CD3OD) | ||
---|---|---|---|---|
δ C | δH Multi (J in Hz) | δ C | δH Multi (J in Hz) | |
1 | 129.8 | 127.0 | ||
2 | 136.9 | 130.1 | ||
3 | 116.9 | 6.60 s | 117.1 | 6.55 s |
4 | 145.1 | 145.5 | ||
5 | 145.3 | 145.7 | ||
6 | 115.7 | 6.72 s | 117.0 | 6.64 s |
7 | 29.0 | 3.86 d (23.0) | 39.6 | 2.83 d (14.5) |
3.62 overlapped | 2.67 d (14.5) | |||
8 | 160.9 | 78.0 | ||
9 | 72.4 | 4.97 d (17.0) | 80.1 | 4.17 d (10.0) |
4.89 d (17.0) | 3.93 d (10.0) | |||
1′ | 123.0 | 135.5 | ||
2′ | 116.2 | 6.59 d (2.0) | 116.0 | 6.58 d (2.0) |
3′ | 145.9 | 146.3 | ||
4′ | 144.6 | 144.8 | ||
5′ | 116.1 | 6.63 d (8.0) | 116.2 | 6.68 d (8.0) |
6′ | 120.3 | 6.45 dd (8.0, 2.0) | 120.2 | 6.52 dd (8.0, 2.0) |
7′ | 42.3 | 4.53 s | 47.4 | 4.18 d (3.0) |
8′ | 128.2 | 56.2 | 3.24 d (3.0) | |
9′ | 173.9 | 181.0 |