| Crystal data |
| Chemical formula |
C2H4N3
+·C2HO4
−
|
|
M
r
|
159.11 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
5.592 (1), 7.2162 (12), 8.4021 (13) |
| α, β, γ (°) |
109.148 (6), 93.889 (7), 103.282 (6) |
|
V (Å3) |
307.92 (9) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.16 |
| Crystal size (mm) |
0.34 × 0.22 × 0.22 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Quest CMOS PHOTON II |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2016 ▸) |
|
T
min, T
max
|
0.638, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
4805, 1524, 1278 |
|
R
int
|
0.038 |
| (sin θ/λ)max (Å−1) |
0.668 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.037, 0.102, 1.07 |
| No. of reflections |
1524 |
| No. of parameters |
112 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.37, −0.20 |
