| Crystal data |
| Chemical formula |
C24H27Cl2NOS |
|
M
r
|
448.42 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
150 |
|
a, b, c (Å) |
8.9961 (3), 10.3755 (3), 13.2565 (4) |
| α, β, γ (°) |
73.857 (1), 88.119 (1), 74.182 (1) |
|
V (Å3) |
1142.32 (6) |
|
Z
|
2 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
3.52 |
| Crystal size (mm) |
0.20 × 0.14 × 0.08 |
| |
| Data collection |
| Diffractometer |
Bruker D8 VENTURE PHOTON 100 CMOS |
| Absorption correction |
Multi-scan (SADABS; Krause et al., 2015 ▸) |
|
T
min, T
max
|
0.54, 0.76 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
8788, 4246, 3772 |
|
R
int
|
0.025 |
| (sin θ/λ)max (Å−1) |
0.618 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.041, 0.107, 1.02 |
| No. of reflections |
4246 |
| No. of parameters |
349 |
| No. of restraints |
14 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.32, −0.50 |
