Table 1.
Data collection and refinement statistics
| Ceg23ΔTM | |
|---|---|
| Data collection | |
| Wavelength (Å) | 0.9798 |
| Resolution range (Å)a | 64.02–2.80 (2.90–2.80) |
| Space group | P 21 21 21 |
| Cell dimensions | |
| a, b, c (Å) | 67.35, 71.61, 142.87 |
| α, β, γ (°) | 90.00, 90.00, 90.00 |
| Total reflections | 223,467 |
| Unique reflections | 17,429 (1654) |
| Multiplicity | 12.8 (13.3) |
| Completeness (%) | 98.76 (96.73) |
| Wilson B-factor | 88.43 |
| Mean I/σ(I) | 14.2 (2.5) |
| Rmerge | 0.122 (0.878) |
| Rmeas | 0.128 (0.912) |
| Rpim | 0.068 (0.246) |
| CC½ | 0.995 (0.901) |
| Anomalous CC | 0.557 (0.005) |
| Refinement | |
| Resolution (Å) | 64.02–2.80 |
| Reflections used in refinement | 17,418 (1655) |
| Rwork | 0.2748 (0.3748) |
| Rfree | 0.2986 (0.3625) |
| Number of nonhydrogen atoms | 4689 |
| Macromolecule atoms | 4689 |
| Solvent | 4 |
| RMS | |
| Bonds (Å) | 0.012 |
| Angles (°) | 0.68 |
| Ramachandran (%) | |
| Favored | 95.76 |
| Allowed | 4.24 |
| Rotamer outliers (%) | 0.00 |
a The values in parentheses are for highest-resolution shell.