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. 2018 Jun 28;16(6):e05286. doi: 10.2903/j.efsa.2018.5286
Substance Minimum recovery per a.s. (90°C, 20 min, pH 4) Minimum recovery per a.s. (100°C, 60 min, pH 5) Minimum recovery per a.s. (120°C, 20 min, pH 6)
1 Aclonifen 96.7 96.8 98.0
2 Amisulbrom 89.9 49.3 11.5
3 Azoxystrobin 100.9 96.2 100.1
4 Beflubutamid 104.4 95.4 98.5
5 Alpha‐Cypermethrin (aka alphamethrin) 99.7 97.6 54.7
6 Benalaxyl 101.0 102.0 98.0
7 Benthiavalicarb 94.8 96.5 93.9
8 Benzovindiflupyr 100.0 100.0 100.0
9 Beta‐Cyfluthrin 106.5 99.7 12.1
10 Bifenthrin 49.0 31.0 81.3
11 Bupirimate 94.9 95.6 91.1
12 Buprofezin 28.2 30.5 76.0
13 Chlorantraniliprole 98.4 85.9 96.2
14 Chlormequat 101.0 99.1  
15 Chlorpyrifos 74.6 19.8 0.8
16 Chromafenozide 94.4    
17 Clopyralid 99.3 96.9 97.1
18 Clothianidin 100.0 100.0 100.0
19 Cyantraniliprole 98.6 98.8 100.2
20 Cyazofamid 18.6 0.0 0.0
21 Cyflumetofen 69.3 5.0 0.0
22 Cymoxanil 11.8
23 Cypermethrin 95.2 96.9 54.7
24 Cyproconazole 96.6 101.0 97.0
25 Cyromazine 99.9 99.1 100.6
26 Deltamethrin 94.8 94.0 25.6
27 Desmedipham 81.8 0.0 0.0
28 Dicamba 100.7 105.1 107.6
29 Diethofencarb 98.8 98.7 98.2
30 Difenoconazole 95.6 96.0 98.6
31 Dimethenamid‐P 96.3 98.6 95.1
32 Dimethomorph 98.1 93.0 99.0
33 Dimoxystrobin 97.7 94.4 0.0
34 Dithianon 28.1 1.0 0.0
35 Dodine 97.1 91.8 94.7
36 Emamectin 84.4 85.9 79.8
37 Epoxiconazole 92.5 97.6 97.6
38 Ethephon 80.5 0.0 0.0
39 Etofenprox 95.6 93.0 94.3
40 Etoxazole 72.2 62.8 59.9
41 Famoxadone 96.2 66.0 43.3
42 Fenamidone 90.1 100.1 102.6
43 Fenazaquin 35.0 61.6 79.4
44 Fenbuconazole 100.7 97.7 104.6
45 Fenhexamid 99.7 95.7 100.2
46 Fenoxycarb 92.2 94.7 95.3
47 Fenpyrazamine 95.1 99.8 89.1
48 Flubendiamide 101.0 100.9 99.8
49 Fluopicolide 98.9 103.8 100.4
50 Fluoxastrobin 95.3 102.6 98.2
51 Flupyradifurone 100.0 100.0 100.0
52 Fluquinconazole 99.0 91.2  
53 Fluxapyroxad 100.0 100.0 100.0
54 Formetanate 88.5 0.6 1.4
55 Fosthiazate 82.6 79.2
56 Hymexazol 100.0 100.0 100.0
57 Imazamox 102.2 103.5 95.2
58 Imidacloprid 97.7 99.2 98.1
59 Indoxacarb 88.0 69.0
60 Iprovalicarb 98.1 97.2 96.9
61 Isofetamid 99.2 97.8 96.8
62 Isopyrazam 96.1 98.6 98.4
63 Lambda‐Cyhalothrin 87.8 82.6 7.8
64 Lufenuron 100.3 95.4 107.2
65 Mandestrobin 94.2 99.8 99.6
66 Mandipropamid 104.9 103.4 109.1
67 Mepanipyrim 101.1 105.7 97.9
68 Mepiquat 95.1 96.6 94.9
69 Metaflumizone 77.0 62.1 89.4
70 Metalaxyl‐M 98.6 100.6 99.3
71 Methoxyfenozide 97.7 95.9 96.1
72 Methomyl 93.7 86.5 58.2
73 Metrafenone 100.5 101.4 94.8
74 Metribuzin 97.6 97.9 97.8
75 Oxamyl 100.0 57.8 0.0
76 Oxathiapiprolin 94.8 94.7 93.8
77 Penconazole 97.3 97.6 97.8
78 Pendimethalin 99.4 99.9 99.2
79 Penflufen 100.9 106.5 99.2
80 Penthiopyrad 101.5 102.1 99.8
81 Phenmedipham 87.3 0.0 0.0
82 Pinoxaden 86.2 72.3 53.5
83 Propiconazole 98.0 99.9 99.6
84 Propineb 62.1 26.4 1.6
85 Proquinazid 95.2 95.9 93.9
86 Prosulfocarb 91.5 94.1 94.6
87 Prothioconazole 99.4 99.9 100.3
88 Pyraclostrobin 98.1 0.0 2.5
89 Pyridaben 97.8 90.0 85.2
90 Pyridalyl 103.4 92.5 95.7
91 Pyriofenone 98.6 98.2 98.3
92 Quinmerac 97.2 103.3 96.2
93 Quizalofop‐P     100.0
94 Sedaxane 98.9 99.4 99.3
95 Spinetoram 94.5 92.1 85.0
96 Spinosad 96.9 95.6 77.5
97 Spirodiclofen 99.1 35.4 37.3
98 Spiromesifen 70.8 13.4 0.9
99 Sulfoxaflor 99.6 100.0 100.4
100 Tau‐Fluvalinate 90.9 40.8 1.7
101 Tebufenozide 100.0 100.0 100.0
102 Tebufenpyrad 100.0 102.4 115.4
103 Tetraconazole 98.7 97.5 97.5
104 Thiacloprid 98.1 96.5 97.0
105 Thiamethoxam 100.0 100.0 98.3
106 Thiencarbazone 36.4 2.6 0.0
107 Thiram 80.3 20.8 0.3
108 Tolclofos‐methyl 61.7 33.6 12.6
109 Triadimenol 96.2 94.4 93.2
110 Triflumuron 98.4 88.9 51.4
111 Trinexapac (aka cimetacarb ethyl) 52.5 58.5 50.9