Table 2. Refinement statistics.
Values in parentheses are for the outer shell.
| Resolution range (Å) | 38.22–2.217 (2.296–2.217) |
| No. of reflections, working set | 15811 |
| No. of reflections, test set | 771 |
| Final R free | 0.2203 |
| Final R cryst | 0.1795 |
| R.m.s. deviations | |
| Bonds (Å) | 0.006 |
| Angles (°) | 0.773 |
| Wilson B factor (Å2) | 26.9 |
| Average B factor (Å2) | 30.0 |
| Ramachandran plot (%) | |
| Most favoured | 96 |
| Outliers | 0.57 |