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. 2020 Jan 8;22(2):80–88. doi: 10.1021/acscombsci.9b00199

Table 1. Screen for the Optimal Equivalences of MgCl2 and NH4Clg.

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a

All reactions were run with 1 nmol of 1a.

b

The percent conversions (% conv.) were determined by LC/MS after the quenching procedure, as described in the Supporting Information.

c

The MS trace was of higher quality relative to that of Trial 6 despite a lower conversion.

d

The MS trace was of higher quality relative to Trial 10.

e,f

The MS signals for those were of lower quality relative to Trial 10.

g

*Catalyst B instead of A. ΔCatalyst B instead of A, reaction time 5 min. ¥Catalyst B instead of A, reaction time 60 min.