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. 2020 Jan 31;5(5):2440–2457. doi: 10.1021/acsomega.9b03989

Table 4. Preparation of Adducts 29a29g by the [4 + 2] Cycloaddition Reactiona.

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a

Reaction conditions: Furan (28) (0.25 mmol), 2-(trimethylsilyl)aryl 4-chlorobenzenesulfonate (7a–7e) (0.375 mmol), CsF (0.75 mmol), and 18-crown-6 ether (0.25 mmol) in PhCN (4 mL) were maintained under stirring at 80 °C for 24 h.

b

Isolated yield.