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Hydroxyl-directed C–H bond activation.a
aIsolated yield.
bReaction conditions: Pd(OAc)2 (10 mol%), PhI (120 mol%), Cs2CO3 (120 mol%), DMF (0.2 M), 100 °C, 24 h.
cReaction conditions: Pd(OAc)2 (10 mol%), ethyl acrylate (200 mol%), 1,4-benzoquinone (100 mol%), HOAc (0.5 M), 80 °C, 24 h.
