Table 1.
Data collection and refinement statistics.
| HsFUT8 in complex with GDP and G0 | |
|---|---|
| Data collection | |
| Space group | C2 |
| Cell dimensions | |
| a, b, c (Å) | 208.04, 68.59, 173.92 |
| α, β, γ (°) | 90, 149.90, 90 |
| Resolution (Å) | 20–1.95 (2.06–1.95)a |
| Rmerge | 0.133 (1.368) |
| I/σI | 6.4 (1.4) |
| Completeness (%) | 99.9 (100) |
| Redundancy | 4.4 (4.5) |
| Refinement | |
| Resolution (Å) | 1.95 |
| No. of reflections | 394,687 |
| Rwork/Rfree | 0.185/0.218 |
| No. of atoms | |
| Protein | 7511 |
| GDP | 56 |
| G0 | 180 |
| Waters | 506 |
| Glycerol | 102 |
| B-factors (Å2) | |
| Protein | 38.11 |
| GDP | 47.64 |
| G0 | 44.70 |
| Waters | 49.00 |
| Glycerol | 63.01 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.0159 |
| Bond angles (°) | 2.0646 |
One crystal was used to determine the crystal structure. aValues in parentheses are for highest-resolution shell.