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. Author manuscript; available in PMC: 2021 Feb 21.
Published in final edited form as: Org Lett. 2020 Feb 11;22(4):1563–1568. doi: 10.1021/acs.orglett.0c00160

Scheme 5.

Scheme 5.

The Reaction of Various 9-Substituted Fluorenes with Alkyl Nitrilesa

aConditions: 5 (0.15 mmol), 2 (1.5 mL, 0.1 M), t-BuOOt-Bu (6 equiv) PivOH (2 equiv), 125 °C, under Ar, 23 h.