Table 2. Intra- and inter-day (n=5) accuracy and precision of QC samples of sumatriptan in plasma.
| Nominal Concentration (ng/mL) | Accuracy (%) | Precision (RSD, %) | ||
|---|---|---|---|---|
| Intra-day | Inter-day | Intra-day | Inter-day | |
| 0.3 (LLOQ) | 95.4 | 99.5 | 7.53 | 11.2 |
| 0.9 (LQC) | 101.1 | 103.2 | 4.74 | 4.99 |
| 30 (MQC) | 102.0 | 102.5 | 2.39 | 2.40 |
| 80 (HQC) | 97.0 | 93.7 | 5.33 | 7.64 |
LQC, low quality control; MQC, middle quality control; HQC, high quality control.