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. 2017 Jun 15;25(2):106–111. doi: 10.12793/tcp.2017.25.2.106

Table 3. Stability of sumatriptan standard in plasma under four different conditions (n=3).

Storage condition LQC (0.9 ng/mL) HQC (80 ng/mL)
Testa Referenceb Testa Referenceb
Post-preparation (24 h at 10 ℃) Mean 0.93 0.89 77.27 76.85
SD (±) 0.02 0.02 2.67 1.45
RSD (%) 2.49 2.25 3.45 1.89
Freeze-thaw cycles (three cycles) Mean 0.90 0.90 72.84 71.86
SD (±) 0.03 0.05 1.80 0.84
RSD (%) 2.94 5.03 2.48 1.16
Short-term (6 h at room temperature) Mean 0.90 0.93 76.31 76.85
SD (±) 0.03 0.02 0.49 1.67
RSD (%) 3.38 1.86 0.64 2.18
Long-term (211 days at −80 ℃) Mean 0.97 0.94 83.40 83.66
SD (±) 0.01 0.01 1.18 0.53
RSD (%) 0.59 1.23 1.41 0.63

aConcentration of samples stored under different storage conditions; bConcentration of freshly prepared samples.