Table V:
Contributions to type B uncertainty
correction | magnitude | uncertainty | explanation |
---|---|---|---|
axial divergence | ≈ −5 | 0.25 | axial fit statistics compared to pooled data statistics (actual value depends on which crystal setup) |
slit height | −0.002 | 0.00 | Δθ = a2 tan θ / (24L2) |
temperature | −6.63 | 0.05 | (t = tlab) – (t = 22.5) lattice parameter shift from crystal lattice reference temperature, limited by 0.02C temp uncertainty |
index of refraction | −2.6 | 0.005 | δ / sin2 θ, limited by form factor uncertainty estimated at 0.2 % |
dynamical asymmetry | 0.015 (1+1), 0.055 (3+3) | 0.01 | previous Monte-Carlo models with copper agree with measured non-dispersive curve. With Mo, non-dispersive curve is too narrow to resolve directly. |
efficiency slope T(E) | 0.03 | 0.05 | from atmospheric pressure 10 % bounds |
angle errors | 0.00 | 0.09 | assuming 0.05″ k=1 uncertainty [15] |
Si d-spacing | 0.00 | 0.03 | in vacuo uncertainty |
Si atmospheric compression | 0.35 | 0.015 | 95 kPa to 105 kPa atmospheric pressure range (extreme limits) |