Table 3.
Isolated yield of syn diastereomer (>20:1 dr) over 3 runs.
Crude yield and dr determined by 1HNMR.
10% Ph2P(O)OH added to increase reactivity.
Isolated yield of syn diastereomer (>20:1 dr) over 3 runs.
Crude yield and dr determined by 1HNMR.
10% Ph2P(O)OH added to increase reactivity.