Table 3.
HRMS data of nusbiarylin compounds.
| Compound | Ion formula | m/z (calculated) | m/z (found) |
|---|---|---|---|
| 1 | C13H15N2O3 [M − H]- | 247.1088 | 247.1089 |
| 2 | C17H11N2O3 [M − H]- | 291.0775 | 291.0773 |
| 3 | C13H9N2O3 [M − H]- | 241.0619 | 241.0620 |
| 4 | C13H8FN2O3 [M − H]- | 259.0524 | 259.0523 |
| 5 | C13H8FN2O3 [M − H]- | 259.0524 | 259.0528 |
| 6 | C13H8FN2O3 [M − H]- | 259.0524 | 259.0522 |
| 7 | C14H11N2O3 [M − H]- | 255.0775 | 255.0771 |
| 8 | C14H11N2O3 [M − H]- | 255.0775 | 255.0772 |
| 9 | C14H11N2O3 [M − H]- | 255.0775 | 255.0772 |
| 10 | C17H17N2O3 [M − H]- | 297.1245 | 297.1247 |
| 11 | C17H17N2O3 [M − H]- | 297.1245 | 297.1242 |
| 12 | C17H17N2O3 [M − H]- | 297.1245 | 297.1243 |
| 13 | C13H9N2O4 [M − H]- | 257.0568 | 257.0565 |
| 14 | C13H9N2O4 [M − H]- | 257.0568 | 257.0568 |
| 15 | C13H9N2O4 [M − H]- | 257.0568 | 257.0567 |
| 16 | C13H8ClN2O3 [M − H]- | 275.0229 | 275.0227 |
| 17 | C13H8ClN2O3 [M − H]- | 275.0229 | 275.0226 |
| 18 | C13H8ClN2O3 [M − H]- | 275.0229 | 275.0226 |
| 19 | C14H11N2O4 [M − H]- | 271.0724 | 271.0719 |
| 20 | C14H11N2O4 [M − H]- | 271.0724 | 271.0721 |
| 21 | C14H11N2O4 [M − H]- | 271.0724 | 271.0727 |
| 22 | C15H11N2O5 [M − H]- | 299.0673 | 299.0672 |
| 23 | C15H11N2O5 [M − H]- | 299.0673 | 299.0669 |
| 24 | C15H11N2O5 [M − H]- | 299.0673 | 299.0672 |
| 25 | C14H8F3N2O3 [M − H]- | 309.0493 | 309.0492 |
| 26 | C14H8F3N2O3 [M − H]- | 309.0493 | 309.0491 |
| 27 | C14H8F3N2O3 [M − H]- | 309.0493 | 309.0490 |
| 28 | C15H9N2O3 [M − H]- | 265.0619 | 265.0618 |
| 29 | C15H9N2O3 [M − H]- | 265.0619 | 265.0620 |
| 30 | C15H9N2O3 [M − H]- | 265.0619 | 265.0615 |
| 31 | C14H11N2O4 [M − H]- | 271.0724 | 271.0721 |
| 32 | C14H11N2O4 [M − H]- | 271.0724 | 271.0722 |
| 33 | C14H9N2O5 [M − H]- | 285.0517 | 285.0513 |
| 34 | C13H17N2O3 [M − H]- | 249.1245 | 249.1245 |
| 35 | C17H13N2O3 [M − H]- | 293.0932 | 293.0929 |
| 36 | C13H11N2O3 [M − H]- | 243.0775 | 243.0775 |
| 37 | C13H10FN2O3 [M − H]- | 261.0681 | 261.0683 |
| 38 | C13H10FN2O3 [M − H]- | 261.0681 | 261.0679 |
| 39 | C13H10FN2O3 [M − H]- | 261.0681 | 261.0682 |
| 40 | C14H13N2O3 [M − H]- | 257.0932 | 257.0928 |
| 41 | C14H13N2O3 [M − H]- | 257.0932 | 257.0928 |
| 42 | C14H13N2O3 [M − H]- | 257.0932 | 257.0927 |
| 43 | C17H19N2O3 [M − H]- | 299.1401 | 299.1401 |
| 44 | C17H19N2O3 [M − H]- | 299.1401 | 299.1399 |
| 45 | C17H19N2O3 [M − H]- | 299.1401 | 299.1404 |
| 46 | C13H11N2O4 [M − H]- | 259.0724 | 259.0723 |
| 47 | C13H11N2O4 [M − H]- | 259.0724 | 259.0723 |
| 48 | C13H10ClN2O3 [M − H]- | 277.0385 | 277.0384 |
| 49 | C13H10ClN2O3 [M − H]- | 277.0385 | 277.0387 |
| 50 | C13H10ClN2O3 [M − H]- | 277.0385 | 277.0386 |
| 51 | C14H13N2O4 [M − H]- | 273.0881 | 273.0878 |
| 52 | C14H13N2O4 [M − H]- | 273.0881 | 273.0876 |
| 53 | C14H13N2O4 [M − H]- | 273.0881 | 273.0881 |
| 54 | C15H13N2O5 [M − H]- | 301.0830 | 301.0833 |
| 55 | C15H13N2O5 [M − H]- | 301.0830 | 301.0831 |
| 56 | C15H13N2O5 [M − H]- | 301.0830 | 301.0826 |
| 57 | C14H10F3N2O3 [M − H]- | 311.0649 | 311.0651 |
| 58 | C14H10F3N2O3 [M − H]- | 311.0649 | 311.0650 |
| 59 | C14H10F3N2O3 [M − H]- | 311.0649 | 311.0654 |
| 60 | C15H11N2O3 [M − H]- | 267.0775 | 267.0773 |
| 61 | C14H13N2O4 [M − H]- | 273.0881 | 273.0879 |
| 62 | C14H11N2O5 [M − H]- | 287.0673 | 287.0673 |
| 63 | C17H12NO3 [M − H]- | 278.0823 | 278.0822 |
| 64 | C15H9FNO [M − H]- | 238.0674 | 238.0672 |
| 65 | C16H9N2O [M − H]- | 245.0720 | 245.0719 |
| 66 | C17H11N2O [M − H]- | 259.0877 | 259.0876 |
| 67 | C16H12NO2 [M − H]- | 258.0874 | 258.0875 |
| 68 | C15H10NO [M − H]- | 220.0768 | 220.0772 |
| 69 | C15H11N2O2 [M + H]+ | 251.0815 | 251.0818 |
| 70 | C16H13N2O3 [M + H]+ | 281.0921 | 281.0922 |
| 71 | C15H9N2O3 [M − H]- | 265.0619 | 265.0620 |
| 72 | C15H9N2O3 [M − H]- | 265.0619 | 265.0616 |
| 73 | C15H9N2O3 [M − H]- | 265.0619 | 265.0621 |
| 74 | C15H8BrN2O3 [M − H]- | 342.9724 | 342.9727 |
| 75 | C15H8Cl2NO [M − H]- | 287.9988 | 287.9987 |
| 76 | C17H14NO3 [M − H]- | 280.0979 | 280.0974 |
| 77 | C15H11FNO [M − H]- | 240.0830 | 240.0829 |
| 78 | C16H11N2O [M − H]- | 247.0877 | 247.0876 |
| 79 | C17H13N2O [M − H]- | 261.1033 | 261.1032 |
| 80 | C16H14NO2 [M − H]- | 252.1030 | 252.1023 |
| 81 | C15H12NO [M − H]- | 222.0924 | 222.0923 |
| 82 | C15H13N2O2 [M + H]+ | 253.0972 | 253.0974 |
| 83 | C16H15N2O3 [M + H]+ | 283.1077 | 283.1080 |
| 84 | C15H11N2O3 [M − H]- | 267.0775 | 267.0773 |
| 85 | C15H11N2O3 [M − H]- | 267.0775 | 267.0770 |
| 86 | C15H10BrN2O3 [M − H]- | 344.9880 | 344.9878 |
| 87 | C15H10Cl2NO [M − H]- | 290.0145 | 290.0141 |
| 88 | C14H10NO3 [M − H]- | 240.0666 | 240.0662 |
| 89 | C15H12NO4 [M − H]- | 270.0772 | 270.0769 |
| 90 | C15H12NO4 [M − H]- | 270.0772 | 270.0771 |
| 91 | C15H9N2O3 [M − H]- | 265.0619 | 265.0617 |
| 92 | C16H12NO5 [M − H]- | 298.0721 | 298.0717 |
| 93 | C16H12NO5 [M − H]- | 298.0721 | 298.0719 |
| 94 | C15H9N2O4 [M − H]- | 281.0568 | 281.0571 |
| 95 | C13H8NO4 [M − H]- | 242.0459 | 242.0454 |