Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C18H18ClN3O2S |
| M r | 375.86 |
| Crystal system, space group | Monoclinic, P21/a |
| Temperature (K) | 298 |
| a, b, c (Å) | 8.9995 (5), 16.7778 (11), 12.3595 (8) |
| β (°) | 98.892 (6) |
| V (Å3) | 1843.8 (2) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.34 |
| Crystal size (mm) | 0.65 × 0.6 × 0.24 |
| Data collection | |
| Diffractometer | Agilent Xcalibur Eos |
| Absorption correction | Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
| T min, T max | 0.857, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 13882, 4340, 3323 |
| R int | 0.027 |
| (sin θ/λ)max (Å−1) | 0.682 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.049, 0.161, 1.10 |
| No. of reflections | 4340 |
| No. of parameters | 230 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.30, −0.41 |