| Crystal data |
| Chemical formula |
C14H36N4
4+·2ClO4
−·2Cl−
|
|
M
r
|
530.27 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
220 |
|
a, b, c (Å) |
7.4990 (15), 8.0790 (16), 9.980 (2) |
| α, β, γ (°) |
81.31 (3), 77.32 (3), 78.39 (3) |
|
V (Å3) |
574.2 (2) |
|
Z
|
1 |
| Radiation type |
Synchrotron, λ = 0.610 Å |
| μ (mm−1) |
0.36 |
| Crystal size (mm) |
0.10 × 0.10 × 0.08 |
| |
| Data collection |
| Diffractometer |
Rayonix MX225HS CCD area detector |
| Absorption correction |
Empirical (using intensity measurements) (HKL3000sm SCALEPACK; Otwinowski & Minor, 1997 ▸) |
|
T
min, T
max
|
0.710, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
6573, 3361, 3208 |
|
R
int
|
0.038 |
| (sin θ/λ)max (Å−1) |
0.706 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.052, 0.147, 1.05 |
| No. of reflections |
3361 |
| No. of parameters |
138 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.97, −0.56 |
