Agilent Xcalibur, Eos diffractometer | 9606 independent reflections |
Radiation source: Enhance (Mo) X-ray Source | 5769 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.063 |
Detector resolution: 16.1593 pixels mm-1 | θmax = 25.0°, θmin = 2.0° |
ω scans | h = −11→11 |
Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014) | k = −15→15 |
Tmin = 0.889, Tmax = 1.000 | l = −17→17 |
9606 measured reflections |