Table 1.
Data collection and refinement statistics.
| PHD:PAF15 (PDB: 6IIW) | |
|---|---|
| Data collection | |
| Beam line | PF-BL17A |
| Wavelength (Å) | 0.98 |
| Space group | P6122 |
| Cell dimensions | |
| a, b, c (Å) | 36.7, 37.6, 220.2 |
| Resolution (Å) | 44.03–1.70 (1.73–1.70)a |
| Rsym or Rmerge (%) | 6.5 (49.7)a |
| I/σ(I) | 27.5 (5.6)a |
| CC1/2 | 99.9 (97.6)a |
| Completeness (%) | 100 (99.9)a |
| Redundancy | 17.2 (17.6)a |
| Unique reflections | 10,762 (538) |
| Refinement | |
| Resolution (Å) | 36.69–1.70 |
| No. of reflections | 10,653 |
| Rwork/Rfree (%) | 17.6/18.9 |
| No. of atoms | |
| PHD | 522 |
| PAF15 | 51 |
| Ion | 4 |
| Water | 96 |
| Average B factors (Å2) | |
| PHD | 26.6 |
| PAF15 | 26.4 |
| Ion | 19.4 |
| Water | 38.4 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.005 |
| Bond angles (°) | 0.928 |
aValues in parentheses are for the highest-resolution shell.