Tab. 2.
Target Reaction | No. | H2O2 Concentration (mmol L−1) | Current (mA) | Na2SO4 concontration (mol L−1) | Electrodea |
---|---|---|---|---|---|
Anodic Oxidation | A1 | 2 | 50 | 0.05 | G+G |
A2 | 2 | 100 | 0.05 | G+G | |
A3 | 2 | 200 | 0.05 | G+G | |
Cathodic Reductionb | C1 | 0.5 | 100 | 0.05 | G+G |
C2 | 2 | 50 | 0.05 | G+G | |
C3 | 2 | 100 | 0.05 | G+G | |
C4 | 2 | 200 | 0.05 | G+G | |
C5 | 10 | 100 | 0.05 | G+G | |
C6 | 2 | 50 | 0.05 | G+R | |
C7 | 2 | 100 | 0.05 | G+R | |
C8 | 2 | 200 | 0.05 | G+R | |
Disproportion in Bulkc | D1 | 0.5 | 200 | 0.01 | G+G |
D2 | 0.5 | 200 | 0.05 | G+G | |
D3 | 0.5 | 200 | 0.25 | G+G | |
D4 | 2 | 200 | 0.01 | G+G | |
D5 | 2 | 200 | 0.05 | G+G | |
D6 | 2 | 200 | 0.25 | G+G | |
D7 | 10 | 200 | 0.01 | G+G | |
D8 | 10 | 200 | 0.05 | G+G | |
D9 | 10 | 200 | 0.25 | G+G |
Note:
G means graphite plate, and R means RVC foam.
pH in the cathodic and anodic compartment was monitored, results were shown in part 3.3.
pH was adjusted to 3.0 for D1~D9, which is the best pH for the EF process [33].