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Tg and storage modulus (E’) obtained from DSC and DMTA experiments. N.d.: not determined.
| Sample | DSC | DMTA | ||
|---|---|---|---|---|
| Tg (°C) run 1 | Tg (°C) run 2 | E’ T = 32 °C (MPa) | Tg (°C) | |
| E0 | 49 | 53 | 1789 ± 15 | 74 ± 0.5 |
| TP | 69 | N.d. | - | - |
| ET5 | 47 | 48 | 1461 ± 114 | 75 ± 3 |
| ET10 | 49 | 46 | 1110 ± 140 | 73 ± 1 |
| ET15 | 49 | 47 | 940 ± 16 | 76 ± 1.5 |
| ET20 | 49 | 43 | 800 ± 73 | 74 ± 3 |
| TGP | 58, 82 | 47, 59 | - | - |
| EP5 | 49 | 48 | 696 ± 25 | 71 ± 1.5 |
| EP10 | 49 | 48 | 232 ± 49 | 77 ± 2 |
| EP15 | 52 | 51 | 149 ± 49; 56 ± 2 | 87 ± 3; 71 ± 3 |
