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. 2020 Feb 10;74(2):161–171. doi: 10.1007/s10858-020-00301-5

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© The Author(s) 2020

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Fig. 2 — a Hyperpolarized H^N-CON correlation spectrum of osteopontin detected in 55 s using hyperpolarized HDO, in ca. 98% deuterated buffer, with assignments of a few well-resolved residues. b conventional reference spectrum acquired in 10% deuterated buffer. c Overlay of the hyperpolarized spectrum (red) and the reference spectrum (black). d Hyperpolarized H^N-CON correlation spectrum of OPN in the presence of 2 equivalents of heparin, with assignments of some well-resolved residues. (Signal intensities are tabulated in Supplementary Tables S2 and S3.)