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The parameter measurements of the XRPD method.
| Geometry | Bragg-Brentano |
|---|---|
| Goniometer radius | 240 mm |
| Radius source | CuKα |
| Generator | 40 kV, 30 mA |
| Tube | Normal focus 10 x 1 mm |
| Divergence and receiving slits | 0.2117O |
| Soller slits | 5.3O |
| Resolving slit | 100 mm |
| Monochromator | Graphite (diffracted beam) |
| Detector | Scintillation counter |
| The scan parameters and step size | 5 - 85O 2θ in 0.020° increments |
| Integration time | 10 s |
