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. Author manuscript; available in PMC: 2020 May 18.
Published in final edited form as: Nat Chem. 2019 Nov 18;11(12):1106–1112. doi: 10.1038/s41557-019-0358-y

Table 1.

NBE Effect for the Alkenyl Catellani Reactiona

graphic file with name nihms-1540634-t0005.jpg
*

Reaction conditions: 1a (0.10 mmol), 2a (0.30 mmol), 3a (0.15 mmol), Pd(cod)Cl2 (0.01 mmol), L1 (0.01 mmol), N (0.15 mmol), 5-trifluomethyl-2-pyridinol (0.02 mmol), Cs2CO3 (0.30 mmol), 100 °C, 16 h. Yield determined by 1H NMR using 1,1,2,2-tetrachloroethane as the internal standard.

a

The conversion was 19%.