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. Author manuscript; available in PMC: 2020 Mar 28.
Published in final edited form as: J Am Chem Soc. 2020 Jan 24;142(10):4793–4799. doi: 10.1021/jacs.9b13757

Table 2.

Control Experimentsa

graphic file with name nihms-1561264-t0010.jpg
entry deviation from “standard conditions” yieldb (%)
1 none >95
2 no 1a <5
3 20 mol% HCpCr(CO)3 or 20 mol% HV(CO)4(dppe) instead of 1a <5
4 1 mol% 1a, 72 h >95
5 0.4 equiv PhSiH3 >95
a

All reactions are performed on 0.5 mmol scale.

b

Determined by 19F NMR.