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. 2010 Feb 6;66(13):2316–2321. doi: 10.1016/j.tet.2010.02.017

Table 1.

Optimization of reaction conditions

graphic file with name fx2.jpg

Entry R1 R2 Ionic liquid Product Reaction time Yield (%)
1 H H [BMIM]Cl 12 h
2 H H [BMIM]BF4 12 h
3 H H [BMIM]BF4–LiCl 3a 20 min 90
4 H H TMGTf 3a 10 min 92
5 Me H [BMIM]Cl 12 h
6 Me H [BMIM]BF4 12 h
7 Me H [BMIM]BF4–LiCl 3b 20 min 92
8 Me H TMGTf 3b 10 min 93