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. Author manuscript; available in PMC: 2020 Aug 17.
Published in final edited form as: Tetrahedron. 2016 Nov 16;72(52):8603–8609. doi: 10.1016/j.tet.2016.11.040

Table 3. Theoretical concentration of samples, average amount of compounds recovered after quantification by sulfur for compounds 4, 5, 6, 7, 8, 9 and 10 in μg/m, % compound recovery and purification methods.

Sample Theoretical concentration (μg compound/mL) Average compound recovery μg compound/mL % compound recovery Purification method
4a 97.80 28.40± 0.725 29.70 HPLC
4b 49.41 15.22± 0.4650 30.80 HPLC
5a 135.6 115.0 ± 1.991 84.80 HPLC
5b 41.70 37.13± 1.112 89.00 HPLC
6 899.4 355.0± 3.098 39.50 SPE
7 1400 50.33± 4.752 3.60 SPE
8 250.0 189.4 75.80 HPLC
9 987.5 49.78 5.00 SPE
10 1228 141.6± 17.36 11.50 SPE

a and b are different concentrations for each sample.