Table 3.

Experimental plan and experimental results after 7 cycles of homogenization in the microfluidizer.

run	P (MPa)	PPI (%)	COR (-)	D[4,3] (nm)	D[3,2] (nm)	Span
1	60	50	2	1215 ± 32	145.0 ± 0.1	3.91 ± 0.09
2	150	50	2	575 ± 27	115.0 ± 0.1	1.2 ± 0.1
3	60	90	2	1178 ± 104	139.0 ± 0.6	3.2 ± 0.5
4	150	90	2	343 ± 35	111.3 ± 0.6	1.85 ± 0.03
5	60	50	4	453 ± 57	114.3 ± 0.5	2.3 ± 0.2
6	150	50	4	222 ± 12	109.3 ± 2.3	1.26 ± 0.06
7	60	90	4	860 ± 65	118.2 ± 0.1	6.0 ± 0.2
8	150	90	4	212 ± 19	109.3 ± 0.5	1.58 ± 0.04
9	60	70	3	654 ± 6	123.0 ± 0.2	2.6 ± 0.1
10	150	70	3	227 ± 10	106.7 ± 2.3	1.6 ± 0.1
11	105	50	3	210 ± 2	112.7 ± 0.6	1.12 ± 0.05
12	105	90	3	252 ± 6	110.0 ± 0.3	1.69 ± 0.01
13	105	70	2	375 ± 18	116.7 ± 0.6	1.15 ± 0.01
14	105	70	4	297 ± 9	109.0 ± 0.1	1.78 ± 0.04
15	105	70	3	268 ± 12	111.0 ± 2.0	2.19 ± 0.09
16	105	70	3	255 ± 4	110.8 ± 0.1	1.73 ± 0.01
17	105	70	3	279 ± 15	112.1 ± 0.2	1.81 ± 0.01
18	105	70	3	250 ± 9	110.3 ± 0.6	1.72 ± 0.02