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. 2006 Jul 27;41(9):1084–1089. doi: 10.1016/j.ejmech.2006.03.024

Scheme 1.

Scheme 1

Synthesis of compounds 521. (a) P(OCH2CH3)3, (n-Bu)4NI, 100–120 °C; (b) methoxy benzaldehyde, NaH, THF, room temperature; (c) BBr3, CH2Cl2, 20–40 °C.