Table 1.
Data collection and refinement statistics (molecular replacement).
| HOIP–HOPIN-1 | HOIP–HOPIN-8 | |
|---|---|---|
| Data collection | ||
| Space group | P212121 | C2 |
| Cell dimensions | ||
| a, b, c (Å) | 39.4, 60.2, 92.3 | 151.6, 88.8, 104.4 |
| α, β, γ (°) | 90, 90, 90 | 90, 101.1, 90 |
| Resolution (Å) | 50–1.54 (1.64–1.54) | 50–2.12 (2.25–2.12) |
| Rmerge | 0.062 (1.580) | 0.117 (1.783) |
| I/σI | 18.22 (1.10) | 9.45 (1.19) |
| Completeness (%) | 99.6 (97.8) | 99.3 (98.6) |
| Redundancy | 8.68 (6.39) | 7.04 (7.20) |
| Refinement | ||
| Resolution (Å) | 46.1–1.54 | 46.59–2.12 |
| No. of reflections | 32,894 | 76,185 |
| Rwork/Rfree | 19.8/21.7 | 21.1/26.7 |
| No. of atoms | ||
| Protein | 1461 | 9385 |
| Ligand/ion | 65 | 285 |
| Water | 127 | 269 |
| B-factors | ||
| Protein | 38.2 | 60.0 |
| Ligand/ion | 46.0 | 61.6 |
| Water | 44.5 | 55.2 |
| R.m.s. deviations | ||
| Bond lengths (Å) | 0.008 | 0.010 |
| Bond angles (°) | 1.445 | 1.183 |
Values in parentheses are for highest-resolution shell.