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. 2006 Oct 12;14(24):8295–8306. doi: 10.1016/j.bmc.2006.09.014

Scheme 1.

Scheme 1

Synthesis of compounds 2a2e. Reagents and conditions: (a) Ph2CCl2, 180 °C, 5 min; (b) O-acetylglycosyl bromide, K2CO3, DMF; (c) 10% Pd/C, H2; (d) i—MeONa, MeOH, ii—H+ resin.