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. 2009 May 15;17(13):4425–4440. doi: 10.1016/j.bmc.2009.05.020

Scheme 2.

Scheme 2

Reagents and conditions: (a) oily anilines added to the diazonium salt solution, followed by CH3COONa; yields: 30–92%; (b) pH 7–8 (1 N NaOH); yields: 25–90%.