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. 2020 Apr 8;11:1736. doi: 10.1038/s41467-020-15556-7

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© The Author(s) 2020

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 3 — ^aSolvent DMF (0.25 mL) + THF (0.5 mL), precursor is sp²-hybridized carbon attached silyl enol ether; ^bPrecursors are highly moisture sensitive; ^cThere was no detected product at 150 and 160 °C; ^dPrecursor 10 mg (0.05 mmol) in DMF (0.3 mL) (n = 4 for RCC); ^etert-Butyldimethylsilyl attached 1-methylimidazole was used as precursor; there was no product detected at 120 °C, 8 min for all reactions.