Table 4.
Recoveries of the nine triterpenoids in P. guajava.
Analyte | Original (mg) | Spike (mg) a | Found (mg) a | Recovery (%) (n = 3) | RSD (%) |
---|---|---|---|---|---|
1 | 1.54 | 1.23 | 2.76 | 99.19 | 1.42 |
1.60 | 3.25 | 106.87 | 1.02 | ||
1.89 | 3.54 | 105.82 | 1.57 | ||
2 | 1.33 | 1.01 | 2.32 | 98.02 | 1.64 |
1.38 | 2.74 | 102.17 | 3.37 | ||
1.60 | 2.90 | 98.12 | 2.60 | ||
3 | 6.81 | 5.50 | 12.45 | 102.55 | 1.67 |
6.80 | 13.70 | 101.32 | 1.24 | ||
8.16 | 14.85 | 98.50 | 3.57 | ||
4 | 0.32 | 0.22 | 0.55 | 104.54 | 1.04 |
0.33 | 0.66 | 103.03 | 1.97 | ||
0.40 | 0.73 | 102.50 | 4.42 | ||
5 | 0.67 | 0.52 | 1.16 | 94.23 | 0.22 |
0.62 | 1.27 | 96.77 | 4.33 | ||
0.81 | 1.46 | 97.53 | 2.49 | ||
6 | 0.51 | 0.35 | 0.85 | 97.14 | 3.80 |
0.52 | 1.05 | 103.84 | 2.74 | ||
0.62 | 1.16 | 104.84 | 8.50 | ||
7 | 1.18 | 0.80 | 1.94 | 95.00 | 0.70 |
1.18 | 2.39 | 102.50 | 1.15 | ||
1.42 | 2.62 | 102.82 | 0.24 | ||
8 | - b | 4.27 | 4.48 | 104.92 | 3.20 |
4.98 | 5.32 | 106.83 | 1.87 | ||
5.55 | 5.85 | 105.41 | 3.51 | ||
9 | 1.77 | 1.50 | 3.30 | 102.00 | 0.73 |
1.79 | 3.58 | 101.69 | 1.32 | ||
2.10 | 3.77 | 95.24 | 0.76 |
a The data is presented as an average of three determinations; b Under the limit of quantitation.