Table 3.
Entry | Catalyst | T (°C) | Additive | Decomposition (%) |
---|---|---|---|---|
1 | IPrAu(III)SbF6-IRMOF-10 | 25 | TMB (10 equiv.) | <5 |
2 | IPrAu(III)PF6-bio-MOF-100 | 25 | TMB (10 equiv.) | <5 |
3 | IPrAu(III)(biphenyl)SbF6 | 25 | TMB (10 equiv.) | 68 |
4 | IPrAu(III)PF6-bio-MOF-100a | 55 | none | <5 |
4 | IPrAu(III)(Me2BPDC)SbF6a | 55 | none | 78 |
See Supplemental Information for general reaction conditions.
CDCl3 used instead of CD2Cl2