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Purified SML10 glycopeptide reaction product analysis. NMR data (600 mHz, 25 ℃) NAc: 2.05/23.4 ppm. Thr x and Thr y are glycosylated with β-GlcNAc. “x” and “y” are used to describe two distinct threonine residues.
| H/C-1 | H/C-2 | H/C-3 | H/C-4 | H/C-5 | H/C-6 | |
|---|---|---|---|---|---|---|
| β-GlcNAc A | 4.56 | 3.69 | 3.55 | 3.45 | 3.44 | 3.76; 3.90 |
| 101.0 | 56.6 | 74.8 | 71.0 | 77.0 | 61.9 | |
| Thr x | 4.52 | 4.31 | 1.18 | |||
| 58.7 | 75.9 | 17.1 | ||||
| Thr y | 4.54 | 4.34 | 1.18 | |||
| 58.7 | 75.9 | 17.1 |
