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. 2020 Mar 20;142(15):7100–7107. doi: 10.1021/jacs.0c00985

Figure 2.

Figure 2

Synthesis and structure of trans-RuCl2(SINpEt)(DPEN) C2 and RuCl(SINpEt)(DPEN) C3. Selected bond lengths (Å) and bond angles (deg) of C2: Ru1–C1, 1.984(3); Ru1–N4, 2.146(3); Ru1–N3, 2.214(2); Ru1–C12, 2.222(3); Ru1–C11, 2.229(2); Ru1–Cl2, 2.4205(7); Ru1–Cl1, 2.4211(7); C11–C12, 1.423(5); C1–Ru1–N4, 103.22(11); C1–Ru1–N3, 172.73(11); N4–Ru1–N3, 78.58(9); C12–Ru1–C11, 37.30(12); Cl2–Ru1–Cl1, 160.63(2). Selected bond lengths (Å) and bond angles (deg) of C3: Ru1–C1, 1.953(9); Ru1–C32, 2.061(9); Ru1–N4, 2.153(7); Ru1–C12, 2.192(8); Ru1–N3, 2.203(7); Ru1–C11, 2.206(7); Ru1–Cl1, 2.549(2); C1–Ru1–C32, 99.3(3); C1–Ru1–N3, 173.8(3); N4–Ru1–N3, 75.5(3); C32–Ru1–Cl1, 160.0(3).