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. Author manuscript; available in PMC: 2021 Feb 6.
Published in final edited form as: Tetrahedron Lett. 2019 Dec 5;61(6):151473. doi: 10.1016/j.tetlet.2019.151473

Scheme 4.

Scheme 4.

Reagents and conditions: (a) lipoxidase type I-B from soybean, 0.01 M borate buffer pH 10.7, rt; (b) TCEP-HCl, rt, 22% (over two steps after HPLC purification and desalting).