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. 2020 Apr 27;10:7070. doi: 10.1038/s41598-020-63983-9

Table 1.

Summary of the KD values of biphasic solvent system (TBME/1-BuOH/ACN/H2O) for the main peaks of G. avellana PEE. Compounds: a: caffeic acid hexoside; b: hydroxymethylfurfural; c: mixture; d: phenyl caffeate; e: cyclo(Arg-Trp); f: hydroxybenzoic acid; g: sinapic acid hexoside; h: benzoic acid.

TBME:n-BuOH: ACN:H2O +0.1% TFA KD Peak a (Rt. 14.5 min) KD Peak b (Rt. 16.9 min) KD Peak c (Rt. 20.1 min) KD Peak d (Rt. 22.8 min) KD Peak e (Rt. 23.7 min) KD Peak h(Rt. 34.8 min)
3:1:1:5 0.24 0.21 0.30 0.89 0.64 2.77
2.75:1.25:1:5 0.43 0.36 0.59 1.46 1.37 4.88
2.2:2.2:0.1:5.5 0.33 0.11 0.79 2.18 2.48 10.07
1.8:1.8:2.1:4.3 1.16 1.13 1.86 2.54 2.99 5.11