Table 4. Structure refinement.
Values in parentheses are for the outer shell.
| Resolution range (Å) | 32.9–1.90 (1.95–1.90) |
| Completeness (%) | 96.63 |
| No. of reflections, working set | 17529 |
| No. of reflections, test set | 952 |
| Final R cryst | 0.229 |
| Final R free | 0.266 |
| Cruickshank DPI | 0.222 |
| No. of non-H atoms | |
| Protein | 2085 |
| Ligand | 0 |
| Water | 256 |
| Total | 2341 |
| R.m.s. deviations | |
| Bonds (Å) | 0.005 |
| Angles (°) | 0.745 |
| Average B factors (Å2) | |
| Protein | 13.1 |
| Water | 19.9 |
| Overall | 13.8 |
| Ramachandran plot | |
| Favored regions (%) | 95.8 |
| Additionally allowed (%) | 4.2 |
| Outliers (%) | 0 |