Table 4. Structure solution and refinement.
Values in parentheses are for the outer shell.
| Resolution range (Å) | 48.51–2.99 (3.17–2.99) |
| Completeness (%) | 97.1 (87.0) |
| No. of reflections, working set | 7427 (1108) |
| No. of reflections, test set | 826 (121) |
| Final R cryst | 0.2612 (0.3363) |
| Final R free | 0.2986 (0.3737) |
| No. of non-H atoms | |
| Protein | 2562 |
| Ion | 0 |
| Ligand | 0 |
| Water | 0 |
| Total | 2562 |
| R.m.s. deviations | |
| Bonds (Å) | 0.006 |
| Angles (°) | 1.00 |
| Average B factors (Å2) | |
| Protein | 64.0 |
| Ion | 0 |
| Ligand | 0 |
| Water | 0 |
| Ramachandran plot | |
| Most favored (%) | 91.46 |
| Allowed (%) | 7.59 |
| Outliers (%) | 0.95 |