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. 2019 Oct 16;29(23):126717. doi: 10.1016/j.bmcl.2019.126717

Scheme 2.

Scheme 2

Reagents and conditions: (a) Montmorillonite in MeCN at RT for 3 d; (b) TFA in DCM at 0 °C → RT for 1 h; (c) EDCI, HOPO and DIPEA in DMF at RT for 24 h.