| Bruker APEXII CCD diffractometer | 2471 reflections with I > 2σ(I) |
| φ and ω scans | Rint = 0.073 |
| Absorption correction: multi-scan (SADABS; Bruker, 2003) | θmax = 27.0°, θmin = 2.1° |
| Tmin = 0.660, Tmax = 0.746 | h = −13→13 |
| 23764 measured reflections | k = −12→12 |
| 4102 independent reflections | l = −24→24 |