Table 2. Experimental details.

Crystal data
Chemical formula	C22H31NO3
M r	357.48
Crystal system, space group	Monoclinic, P21/c
Temperature (K)	150
a, b, c (Å)	17.6928 (7), 13.2512 (5), 8.5916 (3)
β (°)	90.184 (2)
V (Å3)	2014.30 (13)
Z	4
Radiation type	Cu Kα
μ (mm−1)	0.61
Crystal size (mm)	0.25 × 0.17 × 0.10
Data collection
Diffractometer	Bruker D8 VENTURE PHOTON 100 CMOS
Absorption correction	Multi-scan (SADABS; Krause et al., 2015 ▸)
T min, T max	0.82, 0.94
No. of measured, independent and observed [I > 2σ(I)] reflections	14697, 3924, 3044
R int	0.048
(sin θ/λ)max (Å−1)	0.618
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S	0.046, 0.105, 1.07
No. of reflections	3924
No. of parameters	359
H-atom treatment	All H-atom parameters refined
Δρmax, Δρmin (e Å−3)	0.19, −0.18

Computer programs: APEX3 and SAINT (Bruker, 2016 ▸), SHELXT/5 (Sheldrick, 2015a ▸), SHELXL2018/3 (Sheldrick, 2015b ▸), DIAMOND (Brandenburg & Putz, 2012 ▸), SHELXTL (Sheldrick, 2008 ▸) and publCIF (Westrip, 2010 ▸).