Table 5. Hydrogen-bond geometry (Å, °) for 1b .
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| C32—H32⋯O1 | 0.95 | 2.51 | 3.333 (2) | 146 |
| C34—H34⋯O1 | 0.95 | 2.88 | 3.574 (2) | 131 |
| C15—H15⋯O1i | 0.95 | 2.65 | 3.499 (2) | 149 |
| C24—H24⋯O2ii | 0.95 | 2.83 | 3.610 (2) | 140 |
| C54—H54B⋯O2iii | 0.98 | 2.31 | 3.282 (3) | 171 |
| C27—H27A⋯O3 | 0.99 | 2.89 | 3.697 (2) | 140 |
| C6—H6⋯O4iv | 0.95 | 2.68 | 3.557 (2) | 153 |
| C8—H8⋯O4iv | 0.95 | 2.84 | 3.642 (3) | 143 |
| C8—H8⋯O5iv | 0.95 | 2.91 | 3.806 (3) | 157 |
| C48—H48⋯O5v | 0.95 | 2.55 | 3.413 (3) | 151 |
| C6—H6⋯O6iv | 0.95 | 2.54 | 3.325 (2) | 140 |
| C22—H22⋯O6ii | 0.95 | 2.56 | 3.502 (2) | 173 |
| C28—H28A⋯N7 | 0.99 | 2.91 | 3.680 (4) | 135 |
| C29—H29B⋯N7 | 0.99 | 2.72 | 3.554 (4) | 143 |
| C31—H31C⋯N7 | 0.98 | 2.85 | 3.703 (4) | 146 |
| C10—H10⋯N8vi | 0.95 | 2.63 | 3.508 (7) | 154 |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
.