Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C21H15N2 +·C7H5O2 − |
| M r | 416.46 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c (Å) | 9.4693 (4), 8.7384 (3), 24.5049 (9) |
| β (°) | 91.792 (1) |
| V (Å3) | 2026.70 (13) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.39 × 0.28 × 0.17 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2016 ▸) |
| T min, T max | 0.708, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 25446, 3979, 3269 |
| R int | 0.046 |
| (sin θ/λ)max (Å−1) | 0.617 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.041, 0.104, 1.10 |
| No. of reflections | 3979 |
| No. of parameters | 289 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.23, −0.33 |